卡尔费休法测定液态氯乙烯中水含量的研究

采用卡尔费休法测定了液态氯乙烯单体中的水含量。试验确定了采样工具、样品的预处理方式及选用溶剂的最优方案,并进行了精密度与准确度的验证。结果表明卡尔费休法测定液态氯乙烯单体中的水含量准确、快速,可以用来准确、及时地指导生产。     

氮含量对HPD-1双相不锈钢组织及力学性能的影响

通过显微组织观察与力学性能测试研究了氮含量(0.08%~0.22％,质量分数)对HPD-1双相不锈钢硬度、拉伸性能、低温冲击性能及疲劳性能的影响。结果表明,氮含量变化可显著影响试验钢γ/α相比例,当氮含量由0.08％升高到0.22％,γ相含量由38.1％提高至56.5％。α相的硬度由273 HV10提高到343 HV10,γ相的硬度由238 HV10提高到299 HV10,试验钢强度明显提升。氮元素对两相比例和奥氏体相韧性的双重影响导致试验钢低温冲击性能呈先上升后下降的趋势;更高的氮含量抑制疲劳裂纹萌生与拓展,是影响HPD-1双相不锈钢室温疲劳性能的主要因素。撕裂棱是疲劳断口的显著特征。     

退火温度对HA/Ti-24Nb-4Zr复合材料组织与性能的影响

利用放电等离子烧结(SPS)技术制备了HA/Ti-24Nb-4Zr生物复合材料,研究了不同退火温度对复合材料显微组织和力学性能(抗压强度、屈服强度、屈强比、压缩弹性模量)的影响。结果表明,烧结态复合材料主要由β-Ti相、少量初生α-Ti相及HA相组成;随着退火温度的升高,复合材料基体中β-Ti相含量增多且晶粒逐渐长大,针状次生α-Ti相在晶界处和晶内不断析出,HA相结构和含量变化不大;与烧结态相比,不同退火温度处理后的复合材料强度和弹性模量先略微上升后下降,而塑韧性呈不断提高趋势;复合材料在850 ℃退火处理后,抗压强度、屈服强度、屈强比和压缩弹性模量值分别为1507 MPa、1270 MPa、0.84和42 GPa,塑韧性得到明显改善,作为生物医用植入材料具有潜在的应用前景。     

等通道挤压纯铝的冷轧织构与组织演变

研究了冷轧形变量对等通道挤压纯铝的形变织构与显微组织的影响。结果表明：当形变量较小时，冷轧使挤压高纯铝的显微组织分布更加均匀。然而，随着形变量的增加，晶粒由等轴向纤维状转变。织构的演变规律为旋转立方织构和{111}<110>向冷轧织构（铜织构、黄铜织构和S织构）转变，同时出现了R织构。由此可见，等通道挤压变形对高纯铝的冷轧组织和织构存在一定的影响。     

直流配网型混合动力系统在车客渡船上的应用

针对车客渡船动力负荷切换频繁,传统柴油机推进油耗高、排放和噪声大的问题,提出一种基于变速发电机组和超级电容储能装置的直流配网型混合动力系统。目前系统已成功应用于“江苏路渡3011”轮,实船运行数据显示:该混合动力系统不仅能达到较好的节油效果、降低排放,更在操控性、舒适性上优于传统的柴油机推进模式。     

HACCP在浓香菜籽油生产中的应用

为了保障浓香菜籽油的产品质量安全,采用HACCP体系对浓香菜籽油生产全过程进行生物、物理、化学的危害分析,确定关键控制点,制定预防措施,并对生产环节进行有效监控,制定纠偏措施,做好记录管理,为浓香菜籽油的安全生产提供借鉴。     

Effect of annealing atmosphere on the structure and dielectric properties of unfilled tungsten bronze ceramics Ba4PrFe0.5Nb9.5O30

Unfilled tungsten bronze ceramics with the nominal formula Ba₄PrFe_0.5Nb_9.5O₃₀ were synthesized via the standard solid-state sintering route, and the effects of oxygen vacancies on the dielectric and electrical properties were investigated in addition to the structure. Room-temperature X-ray diffraction showed that the N₂-annealed sample had the largest cell volume. Low-temperature spectrum showed that N₂ annealing rendered the dielectric constant and dielectric loss more frequency dispersive, whereas O₂ annealing inhibited the frequency dispersion. The dc conductivity of all the samples originated from the electrons produced in the second ionization of oxygen vacancies and was most likely controlled by a mixed conduction mechanism of the electron and oxygen-vacancy ions. The N₂-annealed sample has the highest dc conductivity owing to its high concentration of oxygen vacancies. The broadening of the Raman lines and the decrease of Raman intensity for the N₂-annealed sample originated from a significant structural disorder. X-ray photoelectron spectra demonstrated that the increased oxygen vacancies caused by the change of valences of Fe and Pr ions contributed to the structural disorder.     

Research on Intelligent Control System of Manipulator Based on Multi Degree of Freedom

Wireless Personal Communications - In order to improve the accuracy and flexibility of forestry robot mechanical arm, the mechanical arm mathematical model is constructed in this paper by...     

Asynchronous control for two‐dimensional hidden Markovian jump systems with partly known mode observation conditional probabilities

This study focuses on the asynchronous control problem for two‐dimensional discrete‐time hidden Markovian jump systems where the mode observation conditional probability matrix is partly known. Considering the original system modes are invisible, the observed modes emitted from an observer serve as an alternative for stability analysis and controller design where a mode observation conditional probability matrix is constructed to characterize the emission between system modes and observed modes. Specially, only partly known information of the mode observation conditional probability matrix is accessible. With the introduction of the free‐connection weighting matrices, the asymptotic mean square stability criterion is firstly derived based on Lyapunov method. This introduction provides a further degree of relaxation and less conservatism is therefore achieved. Secondly, we present synthesis conditions for asynchronous state feedback controller design given in terms of a set of interconnected linear matrix inequalities. Moreover, cluster concept based on the partitions of observed modes is adopted which helps to decrease the number of controllers and simplify the design complexity. A numerical example, regarding the cases with and without clustering of the observed modes, is presented to illustrate the effectiveness of the proposed method.